Bis tri-n-butylammonium pyrophosphate
Web5975-18-8 Bis (tributylammonium) Pyrophosphate Pyrophosphoric Acid, compd. with Tributylamine (1:2) (8CI); Bis (tri-n-butylammonium) Pyrophosphate; N,N-Dibutyl-1-butanamine (Diphosphate); … WebMolar Mass. 363.33. Use. Uses tributylammonium pyrophosphate is an organic intermediate, which has been reported to be useful in the preparation of a base-modified …
Bis tri-n-butylammonium pyrophosphate
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WebJan 1, 2005 · After the addition of 140 μl of tri- n -butylamine and 420 μl of 0.5 M bis (tri- n -butylammonium)pyrophosphate in DMF (0.21 mmol, 1.5 eq.), the solution was stirred at room temperature for a further 10 min. To the reaction was added 2.8 ml of 1% I 2 in pyridine/H 2 O (98:2, v/v), and the solution was stirred at room temperature for 15 min. WebMar 16, 2024 · It is critical to thoroughly dry the tri- n -butylammonium salt of the bisphosphonic acid by repeated coevaporation with anhydrous DMF before use to achieve optimal yields. The proton-decoupled 31 P NMR spectra of 3 – 6 are compared in Fig. S44.
Web关键字搜索批量搜索. 批量下单. 分子砌块. 硼酸硼酸酯; Fragments WebApr 7, 1997 · After 30 min cooling on ice 31 μl POCl 3 was added and the reaction mixture was stirred for 3 h at 0 °C. 2 ml Bis-tri-n-butylammonium pyrophosphate and 200 μl tributylamine was added and the reaction mixture was poured into 0.1 M triethylammonium bicarbonate (TEAB) and loaded on DEAE Sephadex A25 column which was equilibrated …
WebTributylammonium pyrophosphate is a phosphorylating reagent used in the synthesis of modified dNTPs (deoxynucleoside triphosphates) which are important building blocks for … WebBis(tri-n-butylammonium) pyrophosphate: CAS No. : 5975-18-8: Molecular Weight : 548.67: MDL No. : MFCD00136019: Purity/ Specification : Molecular Formula : C 24 H …
WebApr 7, 2010 · Compound Tri-n-butylaminewith free spectra: 37 NMR, 11 FTIR, 2 Raman, 2 Near IR, and 15 MS. ... PYROPHOSPHATE tri-Butylammonium chloride tributylamine, hydrogen tetrafluoroborate(1-) Tributylammonium cation. tributylamine, hydrogen hexafluorophosphate(1-) BIS-(TRI-N-BUTYLAMMONIUM)-HEXAFLUOROSILICATE N …
WebdCTP may be prepared (a) by condensation of a dCMP imidazolidate 3180,3193 or morpholidate 3096 with bis (tri- n -butylammonium) pyrophosphate or (b) by enzymatic phosphorylation of dCDP with ATP. 3192 Phosphorylation of 2′-deoxycytidine with sodium trimetaphosphate yields predominantly 3′-dCTP. 3195 View chapter Purchase book raymond reant parapsychologueWebEnter the email address you signed up with and we'll email you a reset link. raymond realty thaneWebTDP may be prepared (a) by the reaction of 5′- O -tosylthymidine with tris (tetra- n -butylammonium)pyrophosphate, 2981 (b) by successive reactions of 3′- O -benzylthymidine with phosphorylating agents containing protective substituents, 3244 (c) by phosphorylation of TMP with dibenzyl phosphorochloridate 2986 or ATP, 3192 or (d) by … raymond reaseWebKey: UKKKTITYQGAFLZ-UHFFFAOYSA-N. SMILES [P-3].[Bi+3] Properties Chemical formula. Bi P: Molar mass: 239.9 Appearance Black solid Density: g/cm 3: Except where … raymond reaumeWebView 5975-18-8/Bis(tri-n-butylammonium) pyrophosphateinformation and document regarding Tributylammonium pyrophosphate, including NMR, HPLC, LC-MS, UPLC & … raymond reardonWebEnter the email address you signed up with and we'll email you a reset link. raymond rebsamenWebThe bis-(tri-n-butylammonium) pyrophosphate was also dried by removal of pyridine in vacuo. The phosphoromorpholidate was dissolved in pyridine, 5 mL, and added to the vessel containing the pyrophosphate reagent. The reaction was allowed to continue overnight at room temperature. The pyridine was removed in vacuo. raymond reber